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Brookhaven National Laboratory Hits World High in Accurately Measuring Materials' Defects

At Brookhaven National Laboratory (BNL), the tiniest defects in materials can now be measured with the highest accuracy ever achieved — akin to finding a speck of dust in an area the size of the United States. Researchers in the Energy Sciences & Technology Department (ES&T) have developed a technique to measure defects with picometer accuracy, a picometer being a trillionth of a meter.

The research was reported in the December 11 issue of the journal Physical Review Letters. The paper’s authors are Lijun Wu and Yimei Zhu, both of ES&T, and J. Tafto, visiting BNL scientist from the University of Oslo, Norway. The work is also featured in Physical Review FocusScience News ran a feature on the research in their December 2, 2000 issue, and Business News has it in a January issue.

From left, Yimei Zhu, Lijun Wu, and Douglas Gillette, all of the EST Dept.

“Defects are tiny deviations from the normal positions of atoms in materials, and they often control a material’s function,” Zhu said. “For example, certain defects allow a larger current to be transported without resistance in superconductors, or improve the electronic, magnetic and optical properties of semiconductors used in computers or digital equipment. This new technique enables researchers to measure defects with unprecedented accuracy, which is important for designing advanced materials.”

The researchers named the new technique interferometry in coherent electron diffraction.  The method, which requires the use of a one-of-a-kind transmission electron microscope, is complementary to neutron-scattering techniques and x-ray scattering techniques.

Because of its small probe size and high spatial resolution, electron microscopy is particularly suited for the investigation of an extremely tiny area of a material, making it indispensable for research in nanometer-scale science and technology. In this new form of interferometry developed at BNL, electrons from a coherent source of light hit a sample from different directions and form particular "interference" patterns, which can be viewed by a detector. This information is then interpreted by scientists to measure defects in materials.

The BNL researchers’ expertise in materials science coupled with a transmission electron microscope made the new technique possible. Built by JEOL of Tokyo according to Brookhaven researchers’ specifications, the microscope on which the research was performed can magnify samples up to 50 million times. At this magnification, an atom looks as big as a ping pong ball, and a ping pong ball would look as big as the earth. One of the best instruments of its kind in the world, the microscope is tailored for research in solid-state physics, chemistry and biology, as well as materials science.  

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Updated: 07/18/2005

 

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