Soft x-ray spectromicroscopy: progress, trend and future development of
soft x-ray spectromicroscopy facility (SMF) at the NSLS-II
May 20, 2011
Brookhaven National Laboratory, Bldg. 725 Seminar Room
Workshop Chair: K. Kaznatcheev (kaznatch@bnl.gov,
ph. 631-344-7155)
The primary objective of the workshop is to draft a Beamline Development
Proposal for National Synchrotron Light Source II for a soft x-ray
spectromicroscopy facility (SMF beamline) dedicated to the study of the
nanoscale origin of macroscopic (electrical, magnetic and optical)
properties of the matter, and the evolution of the system under relevant
conditions. The beamline is envisioned to have two branches:
(i) high energy resolution soft x-ray branch with an energy-resolving
power of R~25,000 over the energy range 301200 eV dedicated to the
measurement of electronic excitation in nano-compounds by angular resolved
photoelectron spectroscopy with spatial resolution exceeding 100nm (nano-ARPES
and -RIXS), and,
(ii) high spatial (~10nm) resolution STXM/TXM branch with moderate
energy resolving power (R~3000, E~80-2500eV), high on sample flux and
precise control over time and polarization of the photon beam
As such, two branches have complimentary scientific missions:
Spatially resolved ARPES/RIXS branch would aid the study of:
- near Fermi edge band renormalization in nano-compounds
- electronic excitation in novel materials, such as transition metal
oxides, where interplay between electron, spin and orbital degrees of
freedom results in electronic inhomogeneity and nanoscale phase
separations
- novel phenomena, such as the origin of the states inside of
superconducting vortexes
- sub-micron size functional devices (such as CNT field effect
transistors), which are beyond the sensitivity limit of the conventional
PES
STXM/TXM station will be capable
- to image magnetism down to fundamental magnetic length and time
scales with elemental sensitivity in advanced multicomponent materials
- to visualize chemical species distribution and their evolution in
electrochemical reactions in conditions relevant to moderate batteries
and fuel cells operation
- to follow orientation reverse dynamic in liquid crystal optical
switch
- control nanoparticles self assembly
The workshop will provide examples of the research performed at the
different x-ray microscopy facilities, explore experimental and detection
techniques successfully coupled with x-ray microscopy and identify the
needs of the user community for such a beamline.
Speakers
Aaron Bostwick, ALS-LBNL / Chuck Black, BNL-CFN / Yi-De Chuang, ALS-LBNL
/ Peter Fischer, CXRO-LBNL / Adam Hitchcock, McMaster Univ. / Qun Shen,
BNL-PS / Tolek Tyliszczak, ALS-LBNL
Note: for those wishing to attend who Do Not have a valid BNL ID badge:
- Non-US citizens MUST register in the Guest Information System before
May 12:http://www.bnl.gov/guv/gis.asp.
- US citizens MUST send their names to lrogers@bnl.gov by
May 16 for BNL access.
Agenda
| 08:30 - 08:45 |
Workshop Introduction |
Qun Shen, BNL-PS |
| X-Ray Microscopy and Condensed Matter Physics Section: Elio Vescovo, Chair |
| 08:45 - 09:30 |
nano-ARPES: A Path from Graphene to Carbon Nanotube |
Aaron
Bostwick, ALS- LBNL |
| 09:30 - 10:10 |
REIXS: Current Status and Scientific Case
for nano-RIXS |
Yi-De Chuang, ALS-LBNL |
| 10:10 - 10:30 |
Break |
|
| X-Ray Microscopy and Material Science Section: Konstantine Kaznatcheev,
Chair |
| 10:30 - 11:15 |
ALS X-ray Microscopy Activity and Future of STXM: 3D
imaging, fluorescence and total electron yield contrast mechanism,
scattering and reflectivity applied to the study of buried interfaces |
Tolek
Tyliszczak, ALS-LBNL |
| 11:15 - 12:00 |
Nanomagnetism: New Frontier for TXM/STXM |
Peter Fischer, CXRO-LBNL |
| 12:00 - 12:15 |
Break |
|
| X-ray Microscopy and Soft Matter Section: Juergen Thieme, Chair |
| 12:15 - 13:00 |
Toward "at operando" STXM: Fuel Cell Study |
Adam Hitchcock,
McMaster Univ. |
| 13:00 - 13:30 |
Photovoltaic Material and Devices |
Chang-Yong Nam,
BNL-CFN |
|
Workshop
Summary |
Konstantine Kaznatcheev, BNL-PS |
Administrative Contact: Lydia Rogers, telephone:
631-344-4746; email: lrogers@bnl.gov

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