General Lab Information

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Synchrotron Techniques & Methods

« All Techniques

Imaging and Microscopy

Imaging and quantifying the morphology, structure, chemistry, elemental variations, and strain distribution of materials

The Imaging and Microscopy Program at Brookhaven Lab's National Synchrotron Light Source II (NSLS-II) offers specialized tools for imaging and characterizing heterogeneous materials in both 2-D and 3-D. The program provides a suite of imaging techniques, which can be paired with spectroscopic analysis to study features ranging from the millimeter to nanometer regime. The program's scientific focus is highly diverse, and includes studies on nanomaterials, energy conversion, biological structures, and climate science.

Program Beamlines

3-ID HXN

Hard X-ray Nanoprobe

The HXN beamline offers scientists a highly advanced suite of analytical tools for imaging and characterizing complex materials at the nanoscale. HXN provides world-leading spatial resolution, unique detection capabilities, and analytical tools that allow scientists to study the structural, elemental, chemical, and crystalline properties of their samples with an unprecedented level of detail.

5-ID SRX

Submicron Resolution X-ray Spectroscopy

The SRX beamline provides world-leading x-rays for studying complex, natural, and engineered systems using advanced imaging and spectroscopy techniques with sub-micron spatial resolution. The expertise of the SRX staff is aligned with the beamline's diverse user community, which ranges from environmental and life sciences to materials science and energy conversion.

9-ID CDI

Coherent Diffraction Imaging

The extremely high spectral brightness of NSLS-II offers perfect conditions for novel imaging techniques such as coherent diffraction imaging. The Imaging and Microscopy Program is currently developing a beamline using this novel approach to reveal structures in 3-D at extremely high spatial resolution.

18-ID FXI

Full Field X-ray Imaging

The FXI beamline offers advanced capabilities for studying the morphology and oxidation states of dynamic systems in 2-D and 3-D. FXI is specialized in in situ and operando studies of energy storage devices, as well as environmental, biological, and materials science samples.

26-ID-1 ANI
26-ID-2 TXN

Advanced Nanoscale Imaging

Tender X-ray Nanoprobe

The Advanced Nanoscale Imaging (ANI) and Tender X-ray Nanoprobe (TXN) beamlines are designed to deliver optimized photon flux with ultimate beam stability for imaging applications. ANI will provide both monochromatic and polychromatic illuminations whereas TXN will focus on a wide tender energy range. Both beamlines will enable high-throughput and high-resolution imaging emphasizing in-situ/operando compatibilities, providing structural, elemental, chemical and strain characterizations over a wide range of sample systems, including microelectronics, energy storage, and environmental science.

29-ID-1 SXN

Soft X-ray Nanoprobe

The Soft X-ray Nanoprobe (SXN) beamline provides advanced nano-imaging and spectroscopy with high photon flux (250–2500 eV). It enables element analysis from carbon to sulfur and beyond. SXN supports STXM for 2D/3D imaging and ptychography for sub-10 nm resolution. It serves diverse fields, including catalysis, condensed matter physics, and environmental science.

NSLS-II scientists achieved record-breaking resolution to image bacteria down to the resolution of a cell membrane at the Hard X-ray Nanoprobe (HXN) beamline using nanoscale x-ray fluorescence microscopy.

NSLS-II scientists Evan Musterman (left) and Andy Kiss (right) prepare for an experiment on the Submicron Resolution X-ray Spectroscopy (SRX) beamline.

Our Partners

Synchrotron Catalysis Consortium

This partner user group is led by principle investigators from Brookhaven National Laboratory, Columbia University and Stony Brook University. Their mission is to cultivate, support and educate the catalysis user community through partnerships with the TES and QAS beamlines. The SCC provides user support for catalysis users, and collaborates with NSLS-II to develop in situ capabilities for both beamlines.