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[Portions of this work were]/[This work was] performed at Beamline X27A, National Synchrotron Light Source (NSLS), Brookhaven National Laboratory. X27A is supported in part by the U.S. Department of Energy - Geosciences (DE-FG02-92ER14244 to The University of Chicago - CARS) and Brookhaven National Laboratory– Department of Environmental Sciences. Use of the NSLS was supported by the U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences, under Contract No. DE-AC02-98CH10886.